Methyl p-chlorocinnamate
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Post Date:
Dec 18,2019
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Expiry Date:
Dec 17,2020
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Detailed Description:
Cas No. :7560-44-3
CAS No: 7560-44-3
Molecular formula: C10H9ClO2
Molecular weight: 196.5
Melting point: 78-81℃
Packing: 25kg Paper barrel
Assay: ≥99%
Quality: Enterprise standard
Physicochemical property: White Crystalline Powder, it can disolve in ethyl alcohol and diethyl ether, can't disolve in water.
Preparation method: Obtained by reacting chlorocinnamic acid with methanol in the presence of concentrated sulfuric acid.
Application: This product is an organic synthesis intermediate.
Storage condition: Seal in a cool, dry environment.
Stability: If used and stored according to specifications, it will not decompose.
Methyl p-chlorocinnamate is an organic chemical, often used in industry, pharmaceutical industry, etc., obtained by reacting chlorobenzaldehyde with acetic anhydride. The chlorobenzene formaldehyde, acetic anhydride and sodium acetate with reaction 13 h under 180 ℃. After the reaction, it is slightly cold. Pour into the water, filter and wash the filter cake with water. Dissolve the cake repeatedly with ammonia until only a small amount of brownish-yellow sticky remains remain. The ammonium salt solution was filtered, then the chlorocinnamic acid was precipitated out with 3N dilute sulfuric acid, and the product was filtered and dried.
Methyl p-chlorocinnamate is mainly used to synthesize methyl bromomethyl cinnamate from the upstream raw material of the antithrombotic agent ozagrel sodium. The methyl methylanilate was prepared by N- butyl diimide bromide bromide and the total yield was 67%.
Keywords: Methyl p-chlorocinnamate, p-chlorocinnamic acid, 1615-02-7, cinnamic acid
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CAS Registry Number:
7560-44-3
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Synonyms:
;4-Chlorocinnamic acid methyl ester;methyl 3-(4-chlorophenyl)prop-2-enoate;methyl (2E)-3-(4-chlorophenyl)prop-2-enoate;
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Molecular Formula:
C10H9ClO2
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Molecular Weight:
196.6303
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Molecular Structure:
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Safety Description:
S22:Do not inhale dust.;
S24/25:Avoid contact with skin and eyes.;
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Company:
Wuhan LANDMARK Industrial Co., Ltd
[ China ]
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Contact:
Halsey
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Tel:
18062529653
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Fax:
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Email:
Halsey.lmd@gmail.com
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